Facility

RHEED–XPS UHV system

UHV preparation and analysis system centred on electron diffraction and photoelectron spectroscopy.

RHEED–XPS UHV system

About the system

The RHEED–XPS platform is designed for controlled preparation and structural/chemical analysis of ultrathin films, clusters and model materials. Diffraction, energy-loss spectroscopy and XPS can be combined with in-situ deposition and gas exposure.

Experimental methods

  • RHEED: reflection high-energy electron diffraction for surface and thin-film structure
  • RHEELS: reflection high-energy electron energy-loss spectroscopy
  • XPS: X-ray photoelectron spectroscopy for surface composition and chemical states

Further equipment & capabilities

  • Dual-beam Tectra evaporation source and individual metal/oxide evaporators
  • Oxford Applied Research thermal gas cracker
  • Quadrupole mass spectrometer and gas inlet for adsorption and catalytic experiments
  • SPECS ion gun for sample cleaning
  • Rapid sample exchange and sample parking
  • Oxygen-plasma treatment for controlled oxidation

Typical research topics

  • Metal clusters on tungsten, cobalt and cerium oxide supports
  • Bimetallic systems and intermetallic alloys on oxide surfaces
  • Preparation and structure of ultrathin WOx layers
  • Functional layers for biological and gas-sensing applications